Parole chiave: Green Chemistry, Microwave Irradiation, Pectin, Solvent-Free, Article, Infrared Spectroscopy, Microwave Radiation, Synthesis, Thermogravimetry, Fourier Transform Infrared,
Affiliazioni:
*** IBB - CNR *** Institute of Biostructures and Bioimages, National Research Council, 80138 Naples, Italy Department of Industrial Engineering, University of Salerno, 84084 Fisciano (SA), Italy
Riferimenti:
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Kappe, C. O., Controlled microwave heating in modern organic synthesis (2004) Angew. Chem. Int. Ed., 43, pp. 6250-6284
Williams, C. K., Hillmyer, M. A., Polymers from renewable resources: A perspective for a special issue of polymer reviews (2008) Polym. Rev., 48, pp. 1-10
Guilherme, M. R., Moia, T. A., Reis, A. V., Paulino, A. T., Rubira, A. F., Mattoso, L. H. C., Muniz, E. C., Tambourgi, E. B., Synthesis and water absorption transport mechanism of a pH sensitive polymer network structured on vinyl-functionalized pectin (2009) Biomacromolecules, 10, pp. 190-196
Coffin, D. R., Fishman, M. L., Physical and mechanical properties of highly plasticized pectin/starch films (1994) J. Appl. Polym. Sci., 54, pp. 1311-1320
Kaplan, D. L., (1998) Biopolymers from Renewable Resources, , Springer-Verlag: Berlin/Heidelberg, Germany
Thakur, B. R., Singh, R. K., Handa, A. K., Chemistry and uses of pectin\\A review (1997) Crit. Rev. Food Sci. Nutr., 37, pp. 47-73
Mitchel, J. R., Hill, S. E., Ledward, D. A., (1998) Functional Properties of Food Macromolecules, 2nd Ed, , Aspen Publication: Gaithersburg, MA, USA
Filippov, M. P., Practical infrared spectroscopy of pectic substances (1992) Food Hydrocoll., 6, pp. 115-142
Kamnev, A. A., Ptitchkina, N. M., Ristic, M., Shkodina, O. G., Ignatov, V. V., (1995) Spectroscopy of Biological Molecules, pp. 445-446. , Merlin, J. C., Turrell, S., Huvenne, J. P., Eds. Kluwer: Dordrecht, The Netherlands
Zhbankov, R. G., Vibrational spectra and structure of mono-and polysaccharides (1992) J. Mol. Struct., 275, pp. 65-84
Matora, A. V., Korshunova, V. E., Shkodina, O. G., Zhemerichkin, D. A., Ptitchkina, N. M., Morris, E. R., The application of bacterial enzymes for extraction of pectin from pumpkin and sugar beet (1995) Food Hydrocoll., 9, pp. 43-46
Xin, J. Y., Wang, Y., Liu, T., Lin, K., Chang, L., Xia, C. G., Biosynthesis of corn starch palmitate by lipase Novozym 435 (2012) Int. J. Mol. Sci., 13, pp. 7226-7236
Microwave-assisted solvent-free modification of pectin was successfully accomplished, consisting in the esterification of several fatty acids by pectin alcoholic functions. The reaction was performed by simply mixing the reagents with a catalytic amount of the inorganic base (potassium carbonate) and irradiating the obtained mixture with microwaves for a short time (3-6 min). The replacement of the traditional heating with a microwave source allowed the development of a new synthetic protocol which provided increased yield of the final products, since it eliminates the small amount of degraded polysaccharide produced during traditional oil bath heating. The desired esters were fully characterized by FT-IR spectroscopy and thermogravimetric analysis.
Vitiello M, Finamore E, Falanga A, Raieta K, Cantisani M, Galdiero F, Pedone C, Galdiero M, Galdiero S * Fusion in Coq(111 visite) Lecture Notes In Computer Science (ISSN: 0302-9743, 0302-974335404636319783540463634, 0302-974335402975459783540297543), 2001; 2178LNCS: 583-596. Impact Factor:0.415 DettagliEsporta in BibTeXEsporta in EndNote
390 Records (370 escludendo Abstract e Conferenze). Impact factor totale: 1290.866 (1239.433 escludendo Abstract e Conferenze). Impact factor a 5 anni totale: 1314.583 (1261.396 escludendo Abstract e Conferenze).
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