High selectivity in new chiral separations of dansyl amino acids by cyclodextrin derivatives in electrokinetic chromatography
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High selectivity in new chiral separations of dansyl amino acids by cyclodextrin derivatives in electrokinetic chromatography (123 visite)

Cucinotta V, Giuffrida A, Grasso G, Maccarrone G, Messina M, Vecchio G

J Chromatogr A (ISSN: 0021-9673), 2007; 1155(2): 172-179.



Tipo di articolo: Journal Article,

Impact factor: 3.641, Impact factor a 5 anni: 3.737

Url: http://www.scopus.com/inward/record.url?eid=2-s2.0-34250163571&partnerID=40&md5=e61a66cc38ac234250dd5964e036d329

Parole chiave: Amino Acids Derivatives, Chiral Separation, Cyclodextrin Derivatives, Electrokinetic Chromatography, Data Reduction, Ethylendiamine, Alpha Amino Acid, Beta Cyclodextrin, Cysteamine Derivative, Dansyl Chloride, Analytic Method, Article, Chiral Chromatography, Enantiomer, Micellar Electrokinetic Chromatography, Priority Journal, Separation Technique, Micellar Electrokinetic Capillary, Dansyl Compounds, Electrophoresis, Stereoisomerism, Capillary Electrochromatography, Molecular Recognition, Chiral Recognition, Chiral Selectivities, Chiral Selectors, Electrokinetic Chromatographies, Enantio Separations, Enantiomeric Pairs, Low Concentrations, Migration Time, Protonation Equilibrium, Chirality, Chromatographic Analysis, Internet Protocols, Molecular Biology, Organic Acids, Ph Effects, Amination, 2 Aminobutyric Acid, Aspartic Acid, Gamma Cyclodextrin Derivative, Glutamic Acid, Leucine, Methionine, Norleucine, Norvaline, Phenylalanine, Threonine Dehydratase, Amino Acid Substitution, Concentration (parameters), Electrophoretic Mobility, Enantioselectivity, Protein Structure, Proton Transport, Gamma-Cyclodextrins, Hydrogen-Ion Concentration, Sensitivity And Specificity,

Affiliazioni:

*** IBB - CNR ***
Department Chemical Sciences, University of Catania, Viale A. Doria 6, 95125 Catania, Italy
Istituto di Biostrutture e Bioimmagini, CNR, Viale A. Doria 6, 95125 Catania, Italy
Department of Chemical Sciences, University of Catania, Viale Andrea Doria 6, 95125 Catania, Italy


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Enantiomeric pairs of 11 dansyl derivatives of α-amino acids were used as analytes in electrokinetic chromatography to test the ability as chiral selectors of two pure derivatives of β-cyclodextrin: the ethylendiamine derivative in primary position (CDen) and a member of a new class of receptors, the cysteamine-bridged hemispherodextrin THCMH. The selectivity obtained by the presence of the hemispherodextrin, appears particularly promising as shown by the large values of resolution obtained. The importance of a detailed analysis of these data is discussed in terms of suggestions for a rational approach to separation science. © 2007 Elsevier B.V. All rights reserved.
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