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In situ identification of organic components of ink used in books from the 1900s by atmospheric pressure matrix assisted laser desorption ionization mass spectrometry (136 visite)

Giurato P, Candura A, Grasso G, Spoto G

Appl Phys A (ISSN: 0947-8396), 2009 Nov; 97(2): 263-269.

Tipo di articolo: Journal Article,

Impact factor: 1.595

Impact factor a 5 anni: 1.813


Parole chiave: Analytical Techniques, Archaeological Objects, Diagnostic Tools, In-Situ, Laser Desorption, Laser Desorption Ionization, Lithographic Printing, Maldi-Ms, Matrix Deposition, Matrix-Assisted Laser Desorption Ionization Mass Spectrometry, Organic Components, Organic Dye, Sample Surface, Spatially Resolved, Atmospheric Pressure, Biological Materials, Laser Diagnostics, Mass Spectrometers, Atmospheric Ionization,

Url: http://www.scopus.com/inward/record.url?eid=2-s2.0-70349301340&partnerID=40&md5=0ba23e574808a95e9bb81aa2ad7972c9

This paper describes the use of atmospheric pressure/matrix assisted laser desorption ionization-mass spectrometry (AP/MALDI-MS) as a spatially resolved analytical technique for the study of organic components of inks used to print coloured parts of ancient books. The possibility to operate at atmospheric pressure makes MALDI-MS a new in situ micro-destructive diagnostic tool suitable for analysing samples in air, simplifying the investigation of the organic components of artistic and archaeological objects. In this work, several organic dyes and pigments were identified in situ by analysing different coloured areas of books printed in the years 1911 and 1920. The detected colouring materials, which were available since the 1890s, were often identified as a mixture, confirming the typical procedures used in the lithographic printing processes. The matrix deposition and the laser desorption process did not cause visible alteration of the sample surface.
*** IBB - CNR ***

DipietroGroup S.r.l., Via Capuana, 96010, Città Giardino-Melilli, (SR), Italy

Dipartimento di Scienze Chimiche, Università di Catania, Viale A. Doria 6, 95125 Catania, Italy

Istituto Biostrutture e Bioimmagini, CNR, Viale A. Doria 6, 95125 Catania, Italy

DipietroGroup S. r. l., Via Capuana, 96010, Citt Giardino-Melilli, (SR), Italy
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Licciardello, M.P., D'Agata, R., Grasso, G., Simone, S., Spoto, G., (2008) Lasers in the Conservation of Artworks E., pp. 67-72. , Castillejo M. Taylor & Francis Group London 978-0-415-47596-9

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Clark, R. J. H., (2007) J. Mol. Struct., 834, p. 74

Boon, J. J., Learner, T., (2002) J. Anal. Appl. Pyrolysis, 64, p. 327

Grim, D. M., Allison, J., (2004) Archaeometry, 46, p. 283

Licciardello, M. P., D'Agata, R., Grasso, G., Simone, S., Spoto, G., (2008) Lasers in the Conservation of Artworks E., pp. 67-72. , Castillejo M. Taylor & Francis Group London 978-0-415-47596-9

Brunelle, R. L., Pro, M. J., (1972) J. Off. Anal. Chem., 55, p. 823

Brunell, R. L., Cantu, A. A., (1987) J. Forensic Sci., 32, p. 1522

Cantu, A. A., Prough, R. S., (1987) J. Forensic Sci., 32, p. 1151

Aginski, V. N., (1996) Int. J. Forensic Doc. Exam., 2, p. 103

Dunn, J. D., Allison, J., (2007) J. Forensic Sci., 52 (5), pp. 1205-1211

Centeno, S. A., Llad Buisan, V., Ropret, P., (2006) J. Raman Spectrosc., 37, pp. 1111-1118

Wyatt, M. F., Stein, B. K., Brenton, A. G., (2006) Anal. Chem., 78, pp. 199-206

Bamford, C. H., Tipper, C. F. H., (1977), pp. 137-138. , Elsevier AmsterdamGrasso, G., Fragai, M., Rizzarelli, E., Spoto, G., Yeo, K. J., (2007) J. Am. Soc. Mass Spectrom., 18, pp. 961-969

Berkout, V. D., Kryuchkov, S. I., Doroshenko, V. M., (2007) Rapid Commun. Mass Spectrom., 21, pp. 2046-2050

Tan, P. V., Laiko, V. V., Doroshenko, V. M., (2004) Anal. Chem., 76, pp. 2462-2469

Norton, T. H., (1916) Ind. Eng. Chem., 8 (11), pp. 1039-1048

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[Pulisci modulo]
Spoto G, Grasso G
* Spatially resolved mass spectrometry in the study of art and archaeological objects (67 visite)
Trac Trends In Analytical Chemistry (ISSN: 0165-9936), 2011 Jun; 30(6): 856-863.
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Licciardello MP, D'Agata R, Grasso G, Simone S, Spoto G
* Atmospheric Pressure Laser Desorption Mass Spectrometry based methods for the study of traditional painting materials (79 visite)
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D'Agata R, Grasso G, Parlato S, Simone S, Spoto G
* The use of atmospheric pressure laser desorption mass spectrometry for the study of iron-gall ink (99 visite)
Appl Phys A (ISSN: 0947-8396), 2007; 89(1): 91-95.
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Monti SM, Gallo M, Ferracane R, Borrelli RC, Ritieni A, Greco ML, Graniti A, Fogliano V
* Analysis of bacterial lipodepsipeptides by matrix-assisted laser desorption/ionisation time-of-flight and high-performance liquid chromatography with electrospray mass spectrometry (92 visite)
Rapid Commun Mass Spectrom (ISSN: 0951-4198, 1097-0231electronic), 2001; 15(8): 623-628.
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4 Records (4 escludendo Abstract e Conferenze).
Impact factor totale: 10.608 (10.608 escludendo Abstract e Conferenze).
Impact factor a 5 anni totale: 11.243 (11.243 escludendo Abstract e Conferenze).







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