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Collegamenti



The use of atmospheric pressure laser desorption mass spectrometry for the study of iron-gall ink (103 visite)

D'Agata R, Grasso G, Parlato S, Simone S, Spoto G

Appl Phys A (ISSN: 0947-8396), 2007; 89(1): 91-95.

Tipo di articolo: Journal Article,

Impact factor: 1.857

Impact factor a 5 anni: 1.736


Parole chiave: Atmospheric Pressure, Iron, Laser Radiation, Mass Spectrometry, Organic Compounds, Analytical Information, Ancient Works, Archaeological Objects, Iron-Gall Ink,

Url: http://www.scopus.com/inward/record.url?eid=2-s2.0-36048970726&partnerID=40&md5=5c4075c2fabf946a5dc26c0b54863776

The study of ancient works of art is a very challenging task, mainly due to the impossibility of applying experimental approaches that could damage anyhow the object from which analytical information has to be obtained. Spatially resolved analytical methods have significantly enhanced our capacity to study ancient material since they cause minimal and at times no damage to the studied object. Unfortunately, only a few analytical techniques operating within the requested spatial resolution are applicable for the investigation of the organic components of artistic and archaeological objects. In this work, iron-gall ink was prepared according to ancient recipes and its composition was evaluated by AP/MALDI-MS. The latter is demonstrated to be a very valuable tool for the study of the organic components of ancient works of art as it combines the advantages of the vacuum MALDI-MS analytical approach to the possibility of analysing samples in air. In situ analyses were also carried out by analysing strokes of ink directly from paper and parchment. © 2007 Springer-Verlag.
*** IBB - CNR ***

Dipartimento di Scienze Chimiche, Università di Catania, Viale A. Doria 6, Catania 95125, Italy

Dipietro Automazione S.r.l., C. da Cava Sorciaro, Priolo Gargallo (SR), Italy

Istituto Biostrutture e Bioimmagini, CNR, Viale A. Doria 6, Catania 95125, Italy
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Darque-Ceretti, E., Aucouturier, M., (2004) Compr. Anal. Chem., 42, p. 397

Salvado, N., Buti, S., Tobin, M.J., Pantos, E., Prag, A.J.N.W., Pradell, T., (2005) Anal. Chem., 77, p. 3444

Boon, J.J., Learner, T., (2002) J. Anal. Appl. Pyrol., 64, p. 327

Grim, D.M., Allison, J., (2004) Archaeometry, 46, p. 283

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Maier, M.S., Parera, S.D., Seldes, A.M., (2004) Int. J. Mass Spectrosc., 232, p. 225

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Lee, A.S., Mahon, P.J., Creagh, D.C., (2006) Vibr. Spectrosc., 41, p. 170

Mills, J. S., White, R., (1994) The Organic Chemistry of Museum Objects, , Butterworth-Heinemann Oxford

Clark, R. J. H., (2007) J. Mol. Struct., 834, p. 74

Boon, J. J., Learner, T., (2002) J. Anal. Appl. Pyrol., 64, p. 327

Grim, D. M., Allison, J., (2004) Archaeometry, 46, p. 283

Williams, T. I., Saggese, D. A., Wilcox, R. J., Martin, J. D., Muddiman, D. C., (2007) Rapid Commun. Mass Spectrosc., 21, p. 807

Maier, M. S., Parera, S. D., Seldes, A. M., (2004) Int. J. Mass Spectrosc., 232, p. 225

Van Den Berg, J. D. J., Vermist, N. D., Carlyle, L., Hol apek, M., Boon, J. J., (2004) J. Sep. Sci., 28, p. 181

Zumb hl, S., Knochenmuss, R., W lfert, S., Dubois, F., Dale, M. J., Zenobi, R., (1998) Anal. Chem., 70, p. 707

Laiko, V. V., Baldwin, M. A., Burlingame, A. L., (2000) Anal. Chem., 72, p. 652

Schneider, B. B., Lock, C., Covey, T. R., (2005) J. Am. Soc. Mass Spectrosc., 16, p. 176

http: //www. knaw. nl/ecpa/ink/index. html, accessed May 2007 (1992) Plant Polyphenols, , R. W. Hemingway, P. E. Laks (Eds.), (Plenum Press, New York)

Tan, P. V., Laiko, V. V., Doroshenko, V. M., (2004) Anal. Chem., 76, p. 2462

Peterman, S. M., Mulholland, J. J., (2006) J. Am. Soc. Mass Spectrosc., 17, p. 168

Salminen, J. P., Ossipov, V., Loponen, J., Haukioja, E., Pihlaja, K., (1999) J. Chromatogr. A, 864, p. 283

Yadav, M. P., Igartuburu, L. M., Yan, Y., Nothnagel, E. A., (2007) Food Hydrocol., 2, p. 297

Lee, A. S., Mahon, P. J., Creagh, D. C., (2006) Vibr. Spectrosc., 41, p. 170

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13 Records (13 escludendo Abstract e Conferenze).
Impact factor totale: 38.354 (38.354 escludendo Abstract e Conferenze).
Impact factor a 5 anni totale: 41.208 (41.208 escludendo Abstract e Conferenze).







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Ultima modifica di Marco Comerci in data Thursday 19 March 2015, 17:49:28
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