The oxidation of Δ2, Δ2, 4 and Δ4, 6 steroids with RuO4 (386 views)
Steroids (ISSN: 0039-128x), 2004 Mar; 69(3): 173-179.
Export to BibTeX Export to EndNote
Paper type: Journal Article,
Impact factor: 2.337, 5-year impact factor: 2.845
Url: http://www.scopus.com/inward/record.url?eid=2-s2.0-1842638511&partnerID=40&md5=e6e1e4b0dc6d2454aaca3ea03727ad8c
Keywords: α-Ketols, 2-Diols, Oxidation, Ruthenium Tetraoxide, 5 Alpha Androst 2 En 17beta Ol 17 Acetate, Acetic Acid, Alkene, Carboxylic Acid, Cholesta 2, 4 Diene, 6 Dien 3beta Ol 3 Acetate, Hydroxyl Group, Ketone Derivative, Ruthenium Tetroxide, Seco Dicarboxylic Acid, Steroid, Unclassified Drug, Ruthenium Derivative, Article, Cis Isomer, Data Analysis, Energy Yield, Molecular Dynamics, Molecular Interaction, Molecular Mechanics, Oxidation Kinetics, Reaction Analysis, Reduction Kinetics, Ring Opening, Spectroscopy, Stereochemistry, Stoichiometry, Infrared Spectroscopy, Mass Spectrometry, Nuclear Magnetic Resonance Spectroscopy, Oxidation Reduction Reaction, Oxidation-Reduction, Ruthenium Compounds, Fourier Transform Infrared,
Affiliations:
*** IBB - CNR ***
Dipto. di Chim. Organ. e Biochimica, Univ. Studi di Napoli Federico II, Complesso Univ. Monte Sant'Angelo, Via Cinthia, I-80126 Napoli, Italy
References:
Lee, D.G., Van Den Engh, M., The oxidation of organic compounds by ruthenium tetroxide (1973) Oxidation in Organic Chemistry, (PART B), pp. 177-227. , Trahanovsky WS, editor. New York: Academic Pres
Courtney, J.L., Ruthenium tetraoxide oxidations (1986) Organic Syntheses by Oxidation with Metal Compounds, pp. 445-467. , Mijs WJ, de Jonge CRHI, editors. New York, NY: Plenum Press
Lee, D.G., Chen, T., Cleavage reaction (1991) Comprehensive Organic Synthesis, 7, pp. 541-591. , Trost BM, Fleming I, editors. Oxford: Pergamon Press
Naota, T., Takaya, H., Murahashi, S.-I., Ruthenium-catalyzed reactions for organic synthesis (1998) Chem. Rev., 98, pp. 2599-2660
Schröder, M., Osmium tetraoxide cis hydroxylation of unsaturated substrates (1980) Chem. Rev., 80, pp. 187-213
Johnson, R.A., Sharpless, K.B., Catalytic asymmetric dihydroxylation (1993) Catalytic Asymmetric Synthesis, pp. 227-272. , Ojima I, editor. Weinheim: VCH
Romão, C.C., Kühn, F.E., Herrmann, W.A., Rhenium(VII) oxo and imido complexes: Synthesis, structures, and applications (1997) Chem. Rev., 97, pp. 3197-3246
Fatiadi, A.J., The classical permanganate ion: Still a novel oxidant in organic chemistry (1987) Synthesis, pp. 85-127
Piccialli, V., Smaldone, D., Sica, D., Studies towards the synthesis of polyoxygenated steroids. Reaction of some tri- and tetrasubstituted monoene steroids with RuO4 (1993) Tetrahedron, 49, pp. 4211-4228
Notaro, G., Piccialli, V., Sica, D., Smaldone, D., Studies towards the synthesis of polyoxygenated steroids. Reaction of 7,9(11)-diene steroids with RuO4 (1994) Tetrahedron, 50, pp. 4835-4852
Albarella, L., Piccialli, V., Smaldone, D., Sica, D., Ruthenium tetraoxide oxidation of alkenes. Part 7. A more complete picture (1996) J. Chem. Res., (S), pp. 400-401
J. Chem. Res., (M), pp. 2442-2456
Shing, T.K.M., Tam, E.K.W., Tai, V.W.-F., Chung, I.H.F., Jiang, Q., Ruthenium-catalyzed cis-dihydroxylation of alkenes: Scope and limitation (1996) Chem. Eur. J., 2, pp. 50-57
Giordano, F., Piccialli, V., Sica, D., Smaldone, D., Reaction of sterols containing the 7,14- or 8,14-diene system with ruthenium tetraoxide: Formation of epoxysterols (1995) J. Chem. Res., (S), pp. 52-53
Albarella, L., Giordano, F., Lasalvia, M., Piccialli, V., Sica, D., Evidence for the existence of a cyclic ruthenium(VI) diester as an intermediate in the oxidative scission of (-)-α-pinene with RuO 4 (1995) Tetrahedron Lett., 36, pp. 5267-5270
Albarella, L., Lasalvia, M., Piccialli, V., Sica, D., Reaction of RuO4 with carbon-carbon double bonds. Part 8. Reaction of 7,8-didehydrocholesteryl acetate and cholesteryl acetate with RuO4 and OsO4. A comparative view (1998) J. Chem. Soc., Perkin. Trans. 2, pp. 737-743
Carlsen, P.H.J., Katsuki, T., Martin, V.S., Sharpless, K.B., A greatly improved procedure for ruthenium tetroxide catalyzed oxidations of organic compounds (1981) J. Org. Chem., 46, pp. 3936-3938
Albarella, L., Musumeci, D., Sica, D., Reactions of 1,5-dienes with ruthenium tetraoxide: Stereoselective synthesis of tetrahydrofurandiols (2001) Eur. J. Org. Chem., pp. 997-1003
Piccialli, V., RuO4-catalysed oxidative cyclisation of 1,6-dienes to trans-2,6-bis(hydroxymethyl)tetrahydropyran. A novel stereoselective process (2000) Tetrahedron Lett., 41, pp. 3731-3733
Lasalvia, M., Musumeci, D., Piccialli, V., Sica, D., Oxidation of some conjugated diene steroids by hydrogen peroxide, catalysed by methyltrioxorhenium (1998) J. Chem. Res., (S), pp. 694-695
Sica, D., Musumeci, D., Zollo, F., De Marino, S., Reactivity of steroidal dienes towards the methyltrioxorhenium/H 2O2-urea oxidation system: Isolation and characterization of new oxygenated steroids (2001) Eur. J. Org. Chem., pp. 3731-3739
Numazawa, M., Nagaoka, M., Controlled alkaline hydrolysis of steroidal α-bromo ketones: New conditions and synthesis of 2α-hydroxy-3-ones (1982) Steroids, 39, pp. 345-355
Glotter, E., Krinsky-Feibush, P., Rabinsohn, Y., Oxidation of secondary allylic acetates with chromium (VI) reagents (1980) J. Chem. Soc., Perkin. Trans. 1, pp. 1769-1772
Koga, T., Tomoeda, M., Study on conformation and reactivity. VII. The synthesis and transannular cyclization of 2α-hydroxy-5β-cholestane leading to 2α,9α-epoxy-5β-cholestane: A new functionalization reaction at 9C in the steroid nucleus (1970) Tetrahedron, 26, pp. 1043-1059
Suginome, H., Satoh, G., Wang, J.B., Yamada, S., Kobayashi, K., Photoinduced molecular transformations. Part 106. The formation of cyclic anhydrides via regioselective β-scission of alkoxyl radicals generated from 5- and 6-membered α-hydroxy cyclic ketones (1990) J. Chem. Soc., Perkin. Trans. 1, pp. 1239-1245
Lack, R.E., Ridley, A.B., Autoxidation of 2α-hydroxy-5α-cholestan-3-one in methanolic potassium hydroxide (1968) J. Chem. Soc. (C), pp. 3017-3020
Williamson, K.L., Johnson, W.S., Ring-A α-acetoxy ketones in the cholestane series (1961) J. Org. Chem., 26, pp. 4563-4569
Demarco, P.V., Farkas, E., Doddrell, D., Mylari, B.L., Wenkert, E., Pyridine-induced solvent shifts in the nuclear magnetic resonance spectra of hydroxylic compounds (1968) J. Am. Chem. Soc., 90, pp. 5480-5486
Vanantwerp, C.L., Eggert, H., Meakins, G.D., Miners, J.O., Djerassi, C., Additivity relationships in carbon-13 nuclear magnetic resonance spectra of dihydroxy steroids (1977) J. Org. Chem., 42, pp. 789-793
D'Auria, M.V., Minale, L., Riccio, R., Polyoxygenated steroids of marine origin (1993) Chem. Rev., 93, pp. 1839-1895
Migliuolo, A., Piccialli, V., Sica, D., Structure elucidation and synthesis of 3β, 6α-dihydroxy-9-oxo- 9,11-seco-5α-cholest-7-en-11-al, a novel 9,11-secosterol from the sponge Spongia officinalis (1991) Tetrahedron, 47, pp. 7937-7950
Casapullo, A., Minale, L., Zollo, F., Roussakis, C., Verbist, J.F., New cytotoxic polyoxygenated steroids from the sponge Dysidea incrustans (1995) Tetrahedron Lett., 36, pp. 2669-2672
Steroids (ISSN: 0039-128x), 2004 Mar; 69(3): 173-179.
Export to BibTeX Export to EndNote
Paper type: Journal Article,
Impact factor: 2.337, 5-year impact factor: 2.845
Url: http://www.scopus.com/inward/record.url?eid=2-s2.0-1842638511&partnerID=40&md5=e6e1e4b0dc6d2454aaca3ea03727ad8c
Keywords: α-Ketols, 2-Diols, Oxidation, Ruthenium Tetraoxide, 5 Alpha Androst 2 En 17beta Ol 17 Acetate, Acetic Acid, Alkene, Carboxylic Acid, Cholesta 2, 4 Diene, 6 Dien 3beta Ol 3 Acetate, Hydroxyl Group, Ketone Derivative, Ruthenium Tetroxide, Seco Dicarboxylic Acid, Steroid, Unclassified Drug, Ruthenium Derivative, Article, Cis Isomer, Data Analysis, Energy Yield, Molecular Dynamics, Molecular Interaction, Molecular Mechanics, Oxidation Kinetics, Reaction Analysis, Reduction Kinetics, Ring Opening, Spectroscopy, Stereochemistry, Stoichiometry, Infrared Spectroscopy, Mass Spectrometry, Nuclear Magnetic Resonance Spectroscopy, Oxidation Reduction Reaction, Oxidation-Reduction, Ruthenium Compounds, Fourier Transform Infrared,
Affiliations:
*** IBB - CNR ***
Dipto. di Chim. Organ. e Biochimica, Univ. Studi di Napoli Federico II, Complesso Univ. Monte Sant'Angelo, Via Cinthia, I-80126 Napoli, Italy
References:
Lee, D.G., Van Den Engh, M., The oxidation of organic compounds by ruthenium tetroxide (1973) Oxidation in Organic Chemistry, (PART B), pp. 177-227. , Trahanovsky WS, editor. New York: Academic Pres
Courtney, J.L., Ruthenium tetraoxide oxidations (1986) Organic Syntheses by Oxidation with Metal Compounds, pp. 445-467. , Mijs WJ, de Jonge CRHI, editors. New York, NY: Plenum Press
Lee, D.G., Chen, T., Cleavage reaction (1991) Comprehensive Organic Synthesis, 7, pp. 541-591. , Trost BM, Fleming I, editors. Oxford: Pergamon Press
Naota, T., Takaya, H., Murahashi, S.-I., Ruthenium-catalyzed reactions for organic synthesis (1998) Chem. Rev., 98, pp. 2599-2660
Schröder, M., Osmium tetraoxide cis hydroxylation of unsaturated substrates (1980) Chem. Rev., 80, pp. 187-213
Johnson, R.A., Sharpless, K.B., Catalytic asymmetric dihydroxylation (1993) Catalytic Asymmetric Synthesis, pp. 227-272. , Ojima I, editor. Weinheim: VCH
Romão, C.C., Kühn, F.E., Herrmann, W.A., Rhenium(VII) oxo and imido complexes: Synthesis, structures, and applications (1997) Chem. Rev., 97, pp. 3197-3246
Fatiadi, A.J., The classical permanganate ion: Still a novel oxidant in organic chemistry (1987) Synthesis, pp. 85-127
Piccialli, V., Smaldone, D., Sica, D., Studies towards the synthesis of polyoxygenated steroids. Reaction of some tri- and tetrasubstituted monoene steroids with RuO4 (1993) Tetrahedron, 49, pp. 4211-4228
Notaro, G., Piccialli, V., Sica, D., Smaldone, D., Studies towards the synthesis of polyoxygenated steroids. Reaction of 7,9(11)-diene steroids with RuO4 (1994) Tetrahedron, 50, pp. 4835-4852
Albarella, L., Piccialli, V., Smaldone, D., Sica, D., Ruthenium tetraoxide oxidation of alkenes. Part 7. A more complete picture (1996) J. Chem. Res., (S), pp. 400-401
J. Chem. Res., (M), pp. 2442-2456
Shing, T.K.M., Tam, E.K.W., Tai, V.W.-F., Chung, I.H.F., Jiang, Q., Ruthenium-catalyzed cis-dihydroxylation of alkenes: Scope and limitation (1996) Chem. Eur. J., 2, pp. 50-57
Giordano, F., Piccialli, V., Sica, D., Smaldone, D., Reaction of sterols containing the 7,14- or 8,14-diene system with ruthenium tetraoxide: Formation of epoxysterols (1995) J. Chem. Res., (S), pp. 52-53
Albarella, L., Giordano, F., Lasalvia, M., Piccialli, V., Sica, D., Evidence for the existence of a cyclic ruthenium(VI) diester as an intermediate in the oxidative scission of (-)-α-pinene with RuO 4 (1995) Tetrahedron Lett., 36, pp. 5267-5270
Albarella, L., Lasalvia, M., Piccialli, V., Sica, D., Reaction of RuO4 with carbon-carbon double bonds. Part 8. Reaction of 7,8-didehydrocholesteryl acetate and cholesteryl acetate with RuO4 and OsO4. A comparative view (1998) J. Chem. Soc., Perkin. Trans. 2, pp. 737-743
Carlsen, P.H.J., Katsuki, T., Martin, V.S., Sharpless, K.B., A greatly improved procedure for ruthenium tetroxide catalyzed oxidations of organic compounds (1981) J. Org. Chem., 46, pp. 3936-3938
Albarella, L., Musumeci, D., Sica, D., Reactions of 1,5-dienes with ruthenium tetraoxide: Stereoselective synthesis of tetrahydrofurandiols (2001) Eur. J. Org. Chem., pp. 997-1003
Piccialli, V., RuO4-catalysed oxidative cyclisation of 1,6-dienes to trans-2,6-bis(hydroxymethyl)tetrahydropyran. A novel stereoselective process (2000) Tetrahedron Lett., 41, pp. 3731-3733
Lasalvia, M., Musumeci, D., Piccialli, V., Sica, D., Oxidation of some conjugated diene steroids by hydrogen peroxide, catalysed by methyltrioxorhenium (1998) J. Chem. Res., (S), pp. 694-695
Sica, D., Musumeci, D., Zollo, F., De Marino, S., Reactivity of steroidal dienes towards the methyltrioxorhenium/H 2O2-urea oxidation system: Isolation and characterization of new oxygenated steroids (2001) Eur. J. Org. Chem., pp. 3731-3739
Numazawa, M., Nagaoka, M., Controlled alkaline hydrolysis of steroidal α-bromo ketones: New conditions and synthesis of 2α-hydroxy-3-ones (1982) Steroids, 39, pp. 345-355
Glotter, E., Krinsky-Feibush, P., Rabinsohn, Y., Oxidation of secondary allylic acetates with chromium (VI) reagents (1980) J. Chem. Soc., Perkin. Trans. 1, pp. 1769-1772
Koga, T., Tomoeda, M., Study on conformation and reactivity. VII. The synthesis and transannular cyclization of 2α-hydroxy-5β-cholestane leading to 2α,9α-epoxy-5β-cholestane: A new functionalization reaction at 9C in the steroid nucleus (1970) Tetrahedron, 26, pp. 1043-1059
Suginome, H., Satoh, G., Wang, J.B., Yamada, S., Kobayashi, K., Photoinduced molecular transformations. Part 106. The formation of cyclic anhydrides via regioselective β-scission of alkoxyl radicals generated from 5- and 6-membered α-hydroxy cyclic ketones (1990) J. Chem. Soc., Perkin. Trans. 1, pp. 1239-1245
Lack, R.E., Ridley, A.B., Autoxidation of 2α-hydroxy-5α-cholestan-3-one in methanolic potassium hydroxide (1968) J. Chem. Soc. (C), pp. 3017-3020
Williamson, K.L., Johnson, W.S., Ring-A α-acetoxy ketones in the cholestane series (1961) J. Org. Chem., 26, pp. 4563-4569
Demarco, P.V., Farkas, E., Doddrell, D., Mylari, B.L., Wenkert, E., Pyridine-induced solvent shifts in the nuclear magnetic resonance spectra of hydroxylic compounds (1968) J. Am. Chem. Soc., 90, pp. 5480-5486
Vanantwerp, C.L., Eggert, H., Meakins, G.D., Miners, J.O., Djerassi, C., Additivity relationships in carbon-13 nuclear magnetic resonance spectra of dihydroxy steroids (1977) J. Org. Chem., 42, pp. 789-793
D'Auria, M.V., Minale, L., Riccio, R., Polyoxygenated steroids of marine origin (1993) Chem. Rev., 93, pp. 1839-1895
Migliuolo, A., Piccialli, V., Sica, D., Structure elucidation and synthesis of 3β, 6α-dihydroxy-9-oxo- 9,11-seco-5α-cholest-7-en-11-al, a novel 9,11-secosterol from the sponge Spongia officinalis (1991) Tetrahedron, 47, pp. 7937-7950
Casapullo, A., Minale, L., Zollo, F., Roussakis, C., Verbist, J.F., New cytotoxic polyoxygenated steroids from the sponge Dysidea incrustans (1995) Tetrahedron Lett., 36, pp. 2669-2672
The oxidation of Δ2, Δ2, 4 and Δ4, 6 steroids with RuO4
In order to find new ways for the functionalization of the A and B rings of the steroid nucleus, the reaction of 5α-androst-2-en-17β-ol 17-acetate (1), cholesta-2,4-diene (4) and cholesta-4,6-dien-3β-ol 3-acetate (7) was examined using stoichiometric amounts of ruthenium tetraoxide to yield 1,2-cis diols and/or α-hydroxy ketones. The reaction of 5α-cholest-2-en-3-ol 3-acetate (9) with ruthenium tetraoxide was also carried out and afforded, apart from an α-hydroxy ketone, also a diketone and a seco-dicarboxylic acid. The structures of all new steroids, including stereochemical details, were deduced by analysis of spectral data. © 2004 Elsevier Inc. All rights reserved.
In order to find new ways for the functionalization of the A and B rings of the steroid nucleus, the reaction of 5α-androst-2-en-17β-ol 17-acetate (1), cholesta-2,4-diene (4) and cholesta-4,6-dien-3β-ol 3-acetate (7) was examined using stoichiometric amounts of ruthenium tetraoxide to yield 1,2-cis diols and/or α-hydroxy ketones. The reaction of 5α-cholest-2-en-3-ol 3-acetate (9) with ruthenium tetraoxide was also carried out and afforded, apart from an α-hydroxy ketone, also a diketone and a seco-dicarboxylic acid. The structures of all new steroids, including stereochemical details, were deduced by analysis of spectral data. © 2004 Elsevier Inc. All rights reserved.
The oxidation of Δ2, Δ2, 4 and Δ4, 6 steroids with RuO4
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The oxidation of Δ2, Δ2, 4 and Δ4, 6 steroids with RuO4
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Tarallo R, Accardo A, Falanga A, Guarnieri D, Vitiello G, Netti P, D'Errico G, Morelli G, Galdiero S
* Clickable functionalization of liposomes with the gH625 peptide from herpes simplex virus type i for intracellular drug delivery (459 views)
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Impact Factor: 5.925
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Ocak M, Helbok A, Rangger C, Peitl PK, Nock BA, Morelli G, Eek A, Sosabowskijk, Breeman WA, Reubi JC, Decristoforo C
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Impact Factor: 4.991
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Caraci F, Molinaro G, Battaglia G, Giuffrida ML, Riozzi B, Traficante A, Bruno V, Cannella M, Merlo S, Wang X, Heinz BA, Nisenbaum ES, Britton TC, Drago F, Sortino MA, Copani A, Nicoletti F
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Impact Factor: 4.883
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Accardo A, Morisco A, Gianolio E, Tesauro D, Mangiapia G, Radulescu A, Brandt A, Morelli G
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Impact Factor: 1.799
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Accardo A, Morisco A, Tesauro D, Pedone C, Morelli G
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Nardelli A, Castaldi E, Ortosecco G, Speranza A, Storto G, Pace L, Salvatore M
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Impact Factor: 1.172
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Varnäs K, Nyberg S, Halldin C, Varrone A, Takano A, Karlsson P, Andersson J, McCarthy D, Smith M, Pierson ME, Söderström J, Farde L
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Impact Factor: 5.008
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Morisco A, Accardo A, Tesauro D, Palumbo R, Benedetti E, Morelli G
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Maurea S, Mollica C, Imbriaco M, Fusari M, Camera L, Salvatore M
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Impact Factor: 0
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Del Vecchio S, Zannetti A, Iommelli F, Lettieri A, Brunetti A, Salvatore M
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Impact Factor: 1.724
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Del Vecchio S, Zannetti A, Iommelli F, Lettieri A, Brunetti A, Salvatore M
* Molecular imaging of tumor microenvironment: Challenges and perspectives (597 views)
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Impact Factor: 1.724
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Accardo A, Mansi R, Morisco A, Mangiapia G, Paduano L, Tesauro D, Radulescu A, Aurilio M, Aloj L, Arra C, Morelli G
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Chambery A, Severino V, Di Maro A, D'Aniello A, Ruvo M, Parente A
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Impact Factor: 4.106
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La Mendola D, Magrì A, Hansson O, Bonomo RP, Rizzarelli E
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Impact Factor: 3.444
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Morisco A, Accardo A, Gianolio E, Tesauro D, Benedetti E, Morelli G
* Micelles derivatized with octreotide as potential target-selective contrast agents in MRI (432 views)
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Impact Factor: 1.807
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Zaccaro L, Del Gatto A, Pedone C, Saviano M
* Peptides for tumour therapy and diagnosis: current status and future directions (1133 views)
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Impact Factor: 4.708
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Chiechio S, Zammataro M, Morales ME, Busceti CL, Drago F, Th Gereau RW, Copani A, Nicoletti F
* Epigenetic modulation of mGlu2 receptors by histone deacetylase inhibitors in the treatment of inflammatory pain (587 views)
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Impact Factor: 4.531
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Pulcrano M, Camera L, Pagano L, Del Vecchio S, Ferone D, Bodei L, Murgia A, Pace L, Storto G, Paganelli G, Colao A, Salvatore M, Lombardi G, Biondi B
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Aloj L, Aurilio M, Rinaldi V, D'Ambrosio L, Tesauro D, Peitl PK, Maina T, Mansi R, Von Guggenberg E, Joosten L, Sosabowski JK, Breeman WA, De Blois E, Koelewijn S, Melis M, Waser B, Beetschen K, Reubi JC, De Jong M
* The EEE project (449 views)
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Impact Factor: 0
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Mai A, Rotili D, Tarantino D, Ornaghi P, Tosi F, Vicidomini C, Sbardella G, Nebbioso A, Miceli M, Altucci L, Filetici P
* Small-molecule inhibitors of histone acetyltransferase activity: Identification and biological properties (604 views)
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Impact Factor: 5.115
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Cuocolo A, Acampa W, Varrone A, Salvatore M
* Highlights of the Annual Congress of the European Association of Nuclear Medicine, Istanbul, 2005: The incremental value of nuclear medicine for patient management and care (585 views)
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Impact Factor: 4.041
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Marrazzo A, Caraci F, Salinaro ET, Su TP, Copani A, Ronsisvalle G
* Neuroprotective effects of sigma-1 receptor agonists against beta-amyloid-induced toxicity (585 views)
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Impact Factor: 1.995
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Savastano S, Pivonello R, Acampa W, Salvatore M, Lombardi G, Colao A, Fenzi G
* Recombinant thyrotropin-induced orbital uptake of [In-111-diethylenetriamine-pentacetic acid-D-phe(1)]octreotide in a patient with inactive Graves' ophthalmopathy (323 views)
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Impact Factor: 6.02
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D'Auria G, Flores G, Falcigno L, Oliva R, Vacatello M, Corsaro MM, Parrilli M, Paolillo L
* Hyaluronate tetrasaccharide-Cu(II) interaction: A NMR study (312 views)
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Impact Factor: 2.733
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De Luca S, Ulhaq S, Dixon M J, EssexJ, Bradley M
* Solid-phase synthesis of a focused library of trypanothione reductase inhibitors (376 views)
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Impact Factor: 2.326
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Kim KM, Varrone A, Watabe H, Shidahara M, Fujita M, Innis RB, Iida H
* Contribution of scatter and attenuation compensation to SPECT images of nonuniformly distributed brain activities (282 views)
J Nucl Med (ISSN: 0161-5505, 1535-5667, 1535-5667electronic), 2003 Apr; 44(4): 512-519.
Impact Factor: 4.899
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Saracino GA, Improta R, Scalmani G, Barone V
* Absolute pKa determination for carboxylic acids using density functional theory and the polarizable continuum model (275 views)
Chem Phys Lett (ISSN: 0009-2614), 2003; 373(3-4): 411-415.
Impact Factor: 2.438
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Formaggio F, Bonchio M, Crisma M, Peggion C, Mezzato S, Polese A, Barazza A, Antonello S, Maran F, Broxterman QB, Kaptein B, Kamphuis J, Vitale RM, Saviano M, Benedetti E, Toniolo C
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Impact Factor: 4.238
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Aloj L, Panico M, Caracó C, Zannetti A, Del Vecchio S, Di Nuzzo C, Arra C, Morelli G, Tesauro D, De Luca S, Pedone C, Salvatore M
* Radiolabeling approaches for cholecystokinin B receptor imaging (496 views)
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Impact Factor: 2.372
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Romanelli A, Garella I, Menchise V, Iacovino R, Saviano M, Montesarchio D, Didierjean C, Lello PD, Rossi F, Benedetti E
* Crystal-state conformation of Cα, α-dialkylated peptides containing chiral β-homo-residues (519 views)
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Impact Factor: 1.451
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Gatos M, Formaggio F, Crisma M, Valle G, Toniolo C, Bonora GM, Saviano M, Iacovino R, Menchise V, Galdiero S, Pedone C, Benedetti E
Conformational Characterization Of Peptides Rich In The Cycloaliphatic C Alpha, Alpha-Disubstituted Glycine 1-Aminocyclononane-1-Carboxylic Acid (441 views)
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Impact Factor: 1.311
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Crisma M, Formaggio F, Valle G, Toniolo C, Saviano M, Iacovino R, Zaccaro L, Benedetti E
Experimental evidence at atomic resolution for intramolecular N- H···π (phenyl) interactions in a family of amino acid derivatives (418 views)
Biopolymers (ISSN: 0006-3525, 0006-6352, 0006-3525print), 1997; 42(1): 1-6.
Impact Factor: 2.425
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CAPASSO S, SICA F, MAZZARELLA L, BALBONI G, GUERRINI R, SALVADORI S
ACID CATALYSIS IN THE FORMATION OF DIOXOPIPERAZINES FROM PEPTIDES CONTAINING TETRAHYDROISOQUINOLINE-3-CARBOXYLIC ACID AT POSITION-2 (453 views)
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Impact Factor: 1.255
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Pavone V, Lombardi A, D'Auria G, Saviano M, Nastri F, Paolillo L, Di Blasio B, Pedone C
β-Alanine containing peptides: A novel molecular tool for the design of γ-turns (828 views)
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Impact Factor: 2.425
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* T-cells produce acidic niches in lymph nodes to suppress their own effector functions (61 views)
Nat Commun (ISSN: 2041-1723linking, 2041-1723electronic), 2020 Aug 17; 11(1): 4113-4113.
Impact Factor: 12.121
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Tarallo V, Iaccarino E, Cicatiello V, Sanna R, Ruvo M, De Falco S
* Oral Delivery of a Tetrameric Tripeptide Inhibitor of VEGFR1 Suppresses Pathological Choroid Neovascularization (195 views)
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Impact Factor: 2.598
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Korotkyi OH, Vovk AA, Dranitsina AS, Falalyeyeva TM, Dvorshchenko KO, Fagoonee S, Ostapchenko LI
* The influence of probiotic diet and chondroitin sulfate administration on Ptgs2, Tgfb1 and Col2a1 expression in rat knee cartilage during monoiodoacetate-induced osteoarthritis (247 views)
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Impact Factor: 2.863
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Lama A, Annunziata C, Coretti L, Pirozzi C, Di Guida F, Nitrato Izzo A, Cristiano C, Mollica MP, Chiariotti L, Pelagalli A, Lembo F, Meli R, Mattace Raso G
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Impact Factor: 5.078
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Supuran CT, Alterio V, Di Fiore A, D'Ambrosio K, Carta F, Monti SM, De Simone G
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Impact Factor: 8.29
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Di Menna L, Joffe ME, Iacovelli L, Orlando R, Lindsley CW, Mairesse J, Gressèns P, Cannella M, Caraci F, Copani A, Bruno V, Battaglia G, Conn PJ, Nicoletti F
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Impact Factor: 3.383
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Caraci F, Nicoletti F, Copani A
* Metabotropic glutamate receptors: the potential for therapeutic applications in Alzheimer's disease (544 views)
Curr Opin Pharmacol (ISSN: 1471-4892), 2017 Dec 23; 38: 1-7.
Impact Factor: 6.313
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Mishra CB, Kumari S, Angeli A, Monti SM, Buonanno M, Tiwari M, Supuran CT
* Discovery of Benzenesulfonamides with Potent Human Carbonic Anhydrase Inhibitory and Effective Anticonvulsant Action: Design, Synthesis, and Pharmacological Assessment (842 views)
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Impact Factor: 6.253
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Langella E, D'Ambrosio K, D'Ascenzio M, Carradori S, Monti SM, Supuran CT, De Simone G
* A Combined Crystallographic and Theoretical Study Explains the Capability of Carboxylic Acids to Adopt Multiple Binding Modes in the Active Site of Carbonic Anhydrases (336 views)
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Impact Factor: 5.317
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D'Ambrosio K, Carradori S, Monti SM, Buonanno M, Secci D, Vullo D, Supuran CT, De Simone G
* Out of the active site binding pocket for carbonic anhydrase inhibitors (481 views) (PDF 237 views)
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Impact Factor: 6.567
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GrassoG, Magrì A, Bellia F, Pietropaolo A, La Mendola D, Rizzarelli E
* The Copper (ii) And Zinc (ii) Coordination Mode Of Hexxh And Hxxeh Motif In Small Peptides: The Role Of Carboxylate Location And Hydrogen Bonding Network (528 views)
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Impact Factor: 3.444
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Dathan NA, Alterio V, Troiano E, Vullo D, Ludwig M, De Simone G, Supuran CT, Monti SM
* Biochemical Characterization Of The Chloroplastic β-Carbonic Anhydrase From Flaveria Bidentis (l. ) "kuntze" (517 views)
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Impact Factor: 2.332
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Sica F, Pica A, Merlino A, Russo Krauss I, Ercole C, Picone D
* The multiple forms of bovine seminal ribonuclease: Structure and stability of a C-terminal swapped dimer (328 views)
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Impact Factor: 3.341
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Rami M, Dubois L, Parvathaneni NK, Alterio V, van Kuijk SJ, Monti SM, Lambin P, De Simone G, Supuran CT, Winum JY
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Impact Factor: 5.48
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Calce E, Monfregola L, De Luca S
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Impact Factor: 0.825
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Madonna S, Scarponi C, Doti N, Carbone T, Cavani A, Scognamiglio PL, Marasco D, Albanesi C
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Impact Factor: 4.518
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Greco A, Fiumara G, Gargiulo S, Gramanzini M, Brunetti A, Cuocolo A
* High-resolution positron emission tomography/computed tomography imaging of the mouse heart (467 views)
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Impact Factor: 2.871
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Carotenuto A, Cipolletta E, Gomez-Monterrey I, Sala M, Vernieri E, Limatola A, Bertamino A, Musella S, Sorriento D, Grieco P, Trimarco B, Novellino E, Iaccarino G, Campiglia P
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Impact Factor: 3.432
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Roviello GN, Roviello G, Musumeci D, Bucci EM, Pedone C
* Dakin-West reaction on 1-thyminyl acetic acid for the synthesis of 1, 3-bis(1-thyminyl)-2-propanone, a heteroaromatic compound with nucleopeptide-binding properties (439 views)
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Impact Factor: 3.914
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Caraci F, Battaglia G, Sortino MA, Spampinato S, Molinaro G, Copani A, Nicoletti F, Bruno V
* Metabotropic glutamate receptors in neurodegeneration/neuroprotection: Still a hot topic? (647 views)
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Impact Factor: 2.659
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De Simone G, Supuran CT
* (In)organic anions as carbonic anhydrase inhibitors (442 views)
J Chem Res (ISSN: 0162-0134, 1873-3344, 0162-0134print), 2012 Jun; 111: 117-129.
Impact Factor: 3.197
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Caraci F, Spampinato S, Sortino MA, Bosco P, Battaglia G, Bruno V, Drago F, Nicoletti F, Copani A
* Dysfunction of TGF-β1 signaling in Alzheimer's disease: Perspectives for neuroprotection (1289 views)
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Impact Factor: 3.677
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Tarallo R, Accardo A, Falanga A, Guarnieri D, Vitiello G, Netti P, D'Errico G, Morelli G, Galdiero S
* Clickable functionalization of liposomes with the gH625 peptide from herpes simplex virus type i for intracellular drug delivery (459 views)
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Impact Factor: 5.925
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Ocak M, Helbok A, Rangger C, Peitl PK, Nock BA, Morelli G, Eek A, Sosabowskijk, Breeman WA, Reubi JC, Decristoforo C
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Impact Factor: 4.991
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Caraci F, Molinaro G, Battaglia G, Giuffrida ML, Riozzi B, Traficante A, Bruno V, Cannella M, Merlo S, Wang X, Heinz BA, Nisenbaum ES, Britton TC, Drago F, Sortino MA, Copani A, Nicoletti F
* Targeting group II Metabotropic Glutamate (mGlu) receptors for the treatment of psychosis associated with alzheimer's disease: Selective activation of mGlu2 receptors amplifies β-amyloid toxicity in cultured neurons, whereas dual activation of mGlu2 and mGlu3 receptors is neuroprotective (765 views)
Mol Pharmacol (ISSN: 0026-895x), 2011 Mar; 79(3): 618-626.
Impact Factor: 4.883
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Accardo A, Morisco A, Gianolio E, Tesauro D, Mangiapia G, Radulescu A, Brandt A, Morelli G
* Nanoparticles containing octreotide peptides and gadolinium complexes for MRI applications (508 views)
J Pept Sci (ISSN: 1075-2617, 1099-1387, 1075-2617print), 2011 Feb; 17(2): 154-162.
Impact Factor: 1.799
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Accardo A, Morisco A, Tesauro D, Pedone C, Morelli G
* Naposomes: A new class of peptide-derivatized, target-selective multimodal nanoparticles for imaging and therapeutic applications (409 views)
Ther Deliv (ISSN: 2041-5990), 2011 Feb; 2(2): 235-257.
Impact Factor: 0
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Nardelli A, Castaldi E, Ortosecco G, Speranza A, Storto G, Pace L, Salvatore M
* Enhancement of reaction conditions for the radiolabelling of DOTA-peptides with high activities of yttrium-90 (541 views)
Applied Radiation And Isotopes (ISSN: 1872-9800, 0969-8043, 0969-8043linking), 2011 Jan; 69(1): 52-55.
Impact Factor: 1.172
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Varnäs K, Nyberg S, Halldin C, Varrone A, Takano A, Karlsson P, Andersson J, McCarthy D, Smith M, Pierson ME, Söderström J, Farde L
* Quantitative analysis of [11C]AZ10419369 binding to 5-HT 1B receptors in human brain (424 views)
J Cereb Blood Flow Metab (ISSN: 0271-678x), 2011 Jan; 31(1): 113-123.
Impact Factor: 5.008
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Morisco A, Accardo A, Tesauro D, Palumbo R, Benedetti E, Morelli G
* Peptide-labeled supramolecular aggregates as selective doxorubicin carriers for delivery to tumor cells (360 views)
Biopolymers (ISSN: 0006-3525, 0006-6352, 0006-3525print), 2011; 96(1): 88-96.
Impact Factor: 2.87
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Maurea S, Mollica C, Imbriaco M, Fusari M, Camera L, Salvatore M
* Magnetic resonance cholangiography with mangafodipir trisodium in Caroli's disease with pancreas involvement (391 views)
Jop (ISSN: 1590-8577, 1590-0857), 2010 Sep 06; 11(5): 460-463.
Impact Factor: 0
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Del Vecchio S, Zannetti A, Iommelli F, Lettieri A, Brunetti A, Salvatore M
* Molecular imaging of tumor microenvironment (504 views)
Q J Nucl Med Mol Im (ISSN: 1824-4785, 1824-4478, 1824-4785linking), 2010 Jun; 54(3): 243-258.
Impact Factor: 1.724
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Del Vecchio S, Zannetti A, Iommelli F, Lettieri A, Brunetti A, Salvatore M
* Molecular imaging of tumor microenvironment: Challenges and perspectives (597 views)
Q J Nucl Med Mol Im (ISSN: 1824-4785, 1824-4478, 1824-4785linking), 2010 Jun; 54(3): 249-258.
Impact Factor: 1.724
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Accardo A, Mansi R, Morisco A, Mangiapia G, Paduano L, Tesauro D, Radulescu A, Aurilio M, Aloj L, Arra C, Morelli G
* Peptide modified nanocarriers for selective targeting of bombesin receptors (429 views)
Mol Biosyst (ISSN: 1742-206x), 2010 May; 6(5): 878-887.
Impact Factor: 3.825
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Chambery A, Severino V, Di Maro A, D'Aniello A, Ruvo M, Parente A
* Quantification of thyrotropin-releasing hormone by liquid chromatography-electrospray mass spectrometry (487 views)
Amino Acids (ISSN: 0939-4451, 1438-2199, 1438-2199electronic), 2010 Apr; 38(4): 1031-1041.
Impact Factor: 4.106
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La Mendola D, Magrì A, Hansson O, Bonomo RP, Rizzarelli E
* Copper(II) complexes with peptide fragments encompassing the sequence 122-130 of human doppel protein (364 views)
Journal Of Inorganic Biochemistry, 2009 May; 103(5): 758-765.
Impact Factor: 3.444
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Morisco A, Accardo A, Gianolio E, Tesauro D, Benedetti E, Morelli G
* Micelles derivatized with octreotide as potential target-selective contrast agents in MRI (432 views)
J Pept Sci (ISSN: 1075-2617, 1099-1387, 1075-2617print), 2009 Mar; 15(3): 242-250.
Impact Factor: 1.807
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Zaccaro L, Del Gatto A, Pedone C, Saviano M
* Peptides for tumour therapy and diagnosis: current status and future directions (1133 views)
Curr Med Chem (ISSN: 0929-8673, 1875-533x, 1875-533xelectronic), 2009 Mar; 16(7): 780-795.
Impact Factor: 4.708
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Chiechio S, Zammataro M, Morales ME, Busceti CL, Drago F, Th Gereau RW, Copani A, Nicoletti F
* Epigenetic modulation of mGlu2 receptors by histone deacetylase inhibitors in the treatment of inflammatory pain (587 views)
Mol Pharmacol (ISSN: 0026-895x), 2009; 75(5): 1014-1020.
Impact Factor: 4.531
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Pulcrano M, Camera L, Pagano L, Del Vecchio S, Ferone D, Bodei L, Murgia A, Pace L, Storto G, Paganelli G, Colao A, Salvatore M, Lombardi G, Biondi B
* Usefulness of [(111)In-DTPA(0)] octreotide scintigraphy in a family with von Hippel-Lindau disease (360 views)
J Endocrinol Invest (ISSN: 0391-4097, 1720-8386electronic), 2008 Apr; 31(4): 352-359.
Impact Factor: 1.888
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Aloj L, Aurilio M, Rinaldi V, D'Ambrosio L, Tesauro D, Peitl PK, Maina T, Mansi R, Von Guggenberg E, Joosten L, Sosabowski JK, Breeman WA, De Blois E, Koelewijn S, Melis M, Waser B, Beetschen K, Reubi JC, De Jong M
* The EEE project (449 views)
Proc Int Cosm Ray Conf Icrc Universidad Nacional Autonoma De Mexico, 2007; 5(HEPART2): 977-980.
Impact Factor: 0
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Mai A, Rotili D, Tarantino D, Ornaghi P, Tosi F, Vicidomini C, Sbardella G, Nebbioso A, Miceli M, Altucci L, Filetici P
* Small-molecule inhibitors of histone acetyltransferase activity: Identification and biological properties (604 views)
J Med Chem (ISSN: 0022-2623, 1520-4804, 0022-2623print), 2006 Nov 16; 49(23): 6897-6907.
Impact Factor: 5.115
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Cuocolo A, Acampa W, Varrone A, Salvatore M
* Highlights of the Annual Congress of the European Association of Nuclear Medicine, Istanbul, 2005: The incremental value of nuclear medicine for patient management and care (585 views)
Eur J Nucl Med (ISSN: 1619-7070, 1619-7089, 0340-6997), 2006 Mar; 33(3): 360-381.
Impact Factor: 4.041
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Marrazzo A, Caraci F, Salinaro ET, Su TP, Copani A, Ronsisvalle G
* Neuroprotective effects of sigma-1 receptor agonists against beta-amyloid-induced toxicity (585 views)
Neuroreport (ISSN: 0959-4965), 2005 Sep 1; 16(11): 1223-1226.
Impact Factor: 1.995
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Savastano S, Pivonello R, Acampa W, Salvatore M, Lombardi G, Colao A, Fenzi G
* Recombinant thyrotropin-induced orbital uptake of [In-111-diethylenetriamine-pentacetic acid-D-phe(1)]octreotide in a patient with inactive Graves' ophthalmopathy (323 views)
Journal Of Clinical Endocrinology & Metabolism (ISSN: 0021-972x), 2005 Apr; 90(4): 2440-2444.
Impact Factor: 6.02
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D'Auria G, Flores G, Falcigno L, Oliva R, Vacatello M, Corsaro MM, Parrilli M, Paolillo L
* Hyaluronate tetrasaccharide-Cu(II) interaction: A NMR study (312 views)
Biopolymers (ISSN: 0006-3525, 0006-6352, 0006-3525print), 2003 Oct; 70(2): 260-269.
Impact Factor: 2.733
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De Luca S, Ulhaq S, Dixon M J, EssexJ, Bradley M
* Solid-phase synthesis of a focused library of trypanothione reductase inhibitors (376 views)
Tetrahedron Lett (ISSN: 0040-4039), 2003 Apr 7; 44(15): 3195-3197.
Impact Factor: 2.326
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Kim KM, Varrone A, Watabe H, Shidahara M, Fujita M, Innis RB, Iida H
* Contribution of scatter and attenuation compensation to SPECT images of nonuniformly distributed brain activities (282 views)
J Nucl Med (ISSN: 0161-5505, 1535-5667, 1535-5667electronic), 2003 Apr; 44(4): 512-519.
Impact Factor: 4.899
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Saracino GA, Improta R, Scalmani G, Barone V
* Absolute pKa determination for carboxylic acids using density functional theory and the polarizable continuum model (275 views)
Chem Phys Lett (ISSN: 0009-2614), 2003; 373(3-4): 411-415.
Impact Factor: 2.438
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Formaggio F, Bonchio M, Crisma M, Peggion C, Mezzato S, Polese A, Barazza A, Antonello S, Maran F, Broxterman QB, Kaptein B, Kamphuis J, Vitale RM, Saviano M, Benedetti E, Toniolo C
* Nitroxyl peptides as catalysts of enantioselective oxidations (498 views)
Chemistry (ISSN: 0947-6539, 1521-3765, 1521-3765electronic), 2002; 8(1): [d]84-93.
Impact Factor: 4.238
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Aloj L, Panico M, Caracó C, Zannetti A, Del Vecchio S, Di Nuzzo C, Arra C, Morelli G, Tesauro D, De Luca S, Pedone C, Salvatore M
* Radiolabeling approaches for cholecystokinin B receptor imaging (496 views)
Biopolymers (ISSN: 0006-3525, 0006-6352, 0006-3525print), 2002; 66(6): 370-380.
Impact Factor: 2.372
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Romanelli A, Garella I, Menchise V, Iacovino R, Saviano M, Montesarchio D, Didierjean C, Lello PD, Rossi F, Benedetti E
* Crystal-state conformation of Cα, α-dialkylated peptides containing chiral β-homo-residues (519 views)
J Pept Sci (ISSN: 1075-2617, 1099-1387, 1075-2617print), 2001; 7(1): 15-26.
Impact Factor: 1.451
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Gatos M, Formaggio F, Crisma M, Valle G, Toniolo C, Bonora GM, Saviano M, Iacovino R, Menchise V, Galdiero S, Pedone C, Benedetti E
Conformational Characterization Of Peptides Rich In The Cycloaliphatic C Alpha, Alpha-Disubstituted Glycine 1-Aminocyclononane-1-Carboxylic Acid (441 views)
J Pept Sci (ISSN: 1075-2617, 1099-1387, 1075-2617print), 1997 Sep; 3(5): 367-382.
Impact Factor: 1.311
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Crisma M, Formaggio F, Valle G, Toniolo C, Saviano M, Iacovino R, Zaccaro L, Benedetti E
Experimental evidence at atomic resolution for intramolecular N- H···π (phenyl) interactions in a family of amino acid derivatives (418 views)
Biopolymers (ISSN: 0006-3525, 0006-6352, 0006-3525print), 1997; 42(1): 1-6.
Impact Factor: 2.425
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CAPASSO S, SICA F, MAZZARELLA L, BALBONI G, GUERRINI R, SALVADORI S
ACID CATALYSIS IN THE FORMATION OF DIOXOPIPERAZINES FROM PEPTIDES CONTAINING TETRAHYDROISOQUINOLINE-3-CARBOXYLIC ACID AT POSITION-2 (453 views)
Int J Pept Protein Res (ISSN: 0367-8377, 0367-8377print), 1995 Jun; 45(6): 567-573.
Impact Factor: 1.255
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Pavone V, Lombardi A, D'Auria G, Saviano M, Nastri F, Paolillo L, Di Blasio B, Pedone C
β-Alanine containing peptides: A novel molecular tool for the design of γ-turns (828 views)
Biopolymers (ISSN: 0006-3525, 0006-6352, 0006-3525print), 1992 Feb; 32(2): 173-184.
Impact Factor: 2.425
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56 Records (56 excluding Abstracts).
Total impact factor: 197.922 (197.922 excluding Abstracts).
Total 5 year impact factor: 185.587 (185.587 excluding Abstracts).
Total impact factor: 197.922 (197.922 excluding Abstracts).
Total 5 year impact factor: 185.587 (185.587 excluding Abstracts).
386 views. Last view on Saturday 14 January 2023, 17:23:04
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