Solvent-Free Synthesis of Modified Pectin Compounds Promoted by Microwave Irradiation (549 views)
Molecules (ISSN: 1420-3049, 1420-3049electronic, 1420-3049linking), 2012 Oct; 17(10): 12234-12242.
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Paper type: Journal Article
Impact factor: 2.428, 5-year impact factor: 2.679
Url: http://www.scopus.com/inward/record.url?eid=2-s2.0-84868112194&partnerID=40&md5=26e6b641f5675e233bb9bd2040d2904f
Keywords: Green Chemistry, Microwave Irradiation, Pectin, Solvent-Free, Article, Infrared Spectroscopy, Microwave Radiation, Synthesis, Thermogravimetry, Fourier Transform Infrared
Affiliations:
*** IBB - CNR ***
Institute of Biostructures and Bioimages, National Research Council, 80138 Naples, Italy
Department of Industrial Engineering, University of Salerno, 84084 Fisciano (SA), Italy
References:
Not available.
Molecules (ISSN: 1420-3049, 1420-3049electronic, 1420-3049linking), 2012 Oct; 17(10): 12234-12242.
Export to BibTeX Export to EndNote
Paper type: Journal Article
Impact factor: 2.428, 5-year impact factor: 2.679
Url: http://www.scopus.com/inward/record.url?eid=2-s2.0-84868112194&partnerID=40&md5=26e6b641f5675e233bb9bd2040d2904f
Keywords: Green Chemistry, Microwave Irradiation, Pectin, Solvent-Free, Article, Infrared Spectroscopy, Microwave Radiation, Synthesis, Thermogravimetry, Fourier Transform Infrared
Affiliations:
*** IBB - CNR ***
Institute of Biostructures and Bioimages, National Research Council, 80138 Naples, Italy
Department of Industrial Engineering, University of Salerno, 84084 Fisciano (SA), Italy
References:
Not available.
Solvent-Free Synthesis of Modified Pectin Compounds Promoted by Microwave Irradiation
Microwave-assisted solvent-free modification of pectin was successfully accomplished, consisting in the esterification of several fatty acids by pectin alcoholic functions. The reaction was performed by simply mixing the reagents with a catalytic amount of the inorganic base (potassium carbonate) and irradiating the obtained mixture with microwaves for a short time (3-6 min). The replacement of the traditional heating with a microwave source allowed the development of a new synthetic protocol which provided increased yield of the final products, since it eliminates the small amount of degraded polysaccharide produced during traditional oil bath heating. The desired esters were fully characterized by FT-IR spectroscopy and thermogravimetric analysis.
Microwave-assisted solvent-free modification of pectin was successfully accomplished, consisting in the esterification of several fatty acids by pectin alcoholic functions. The reaction was performed by simply mixing the reagents with a catalytic amount of the inorganic base (potassium carbonate) and irradiating the obtained mixture with microwaves for a short time (3-6 min). The replacement of the traditional heating with a microwave source allowed the development of a new synthetic protocol which provided increased yield of the final products, since it eliminates the small amount of degraded polysaccharide produced during traditional oil bath heating. The desired esters were fully characterized by FT-IR spectroscopy and thermogravimetric analysis.
Solvent-Free Synthesis of Modified Pectin Compounds Promoted by Microwave Irradiation
| ▼ Chemical modification of natural molecules, such as peptides and polysaccharides, to be employed as therapeutic agents as well as sensor diagnostic tools |
Solvent-Free Synthesis of Modified Pectin Compounds Promoted by Microwave Irradiation
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View Export to BibTeX Export to EndNote
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View Export to BibTeX Export to EndNote
26 Records (25 excluding Abstracts).
Total impact factor: 106.963 (102.612 excluding Abstracts).
Total 5 year impact factor: 97.271 (92.888 excluding Abstracts).
Total impact factor: 106.963 (102.612 excluding Abstracts).
Total 5 year impact factor: 97.271 (92.888 excluding Abstracts).
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